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论文编号:ZY059 论文字数:9467,页数:36
摘 要:本文以文献资料和小试实验数据为依据,结合工艺设备要求,进行了年产量为100吨的N-叔丁氧羰基-4(R)-羟基-L-脯氨酸的工艺设计。通过三种工艺方法比较,确定了适宜的工艺路线。针对所选定的工艺路线,进行了物料衡算和能量衡算;对主要设备进行了设备选型,环境保护;绘制车间设备布置图。
关键词:N-叔丁氧羰基羟脯氨酸;物料衡算;能量衡算;工艺设计
Abstract: In this paper, the design on pilot-technology is based on literatures and dates of lab trail,combined with the technical equipment requirements, carried out with annual output of 100 tons of N-tert-Boutoxycarbonyl hydroxyproline in the process design.Comparison of three methods of process, determine the appropriate process route. Flow of the routes for the selected,conducted mass balance and energy balance, the main equipment of the equipment selection,environmental protection,draw the workshop equipment layout.
Keywords:N-tert-Boutoxycarbonyl hydroxyproline; Material Balance; Energy Balance; Process Design
目 录
中文摘要............................................................. I
英文摘要............................................................ II
目录............................................................... III
1. 绪论
1.1 概述 .......................................................1
2. 生产流程的确定
2.1 各种方法的比较..............................................4
3. BHO工艺合成书
3.1 设计内容....................................................6
3.2 流程简介...............................................6
3.3 生产周期的确定..............................................6
3.4 年产100吨BHO的物料衡算.....................................7
3.5 热量衡算...................................................11
4 主要设备的选型
4.1 主要设备的选型.............................................24
4.2 设备的选型.................................................25
5 工作总结
5.1 物料衡算结果...............................................26
5.2 热量衡算结果...............................................27
5.3 设备的选型.................................................28
6 三废的处理
6.1 废气处理...................................................30
6.2 废渣处理...................................................30
6.3 废液处理...................................................30
致谢................................................................31
参考文献............................................................32